2-甲基-1-(三甲基硅杂氧基)-1-丙烯合成路线 （共 23 条）
反应条件
triethylamine; potassium iodide in N,N-dimethyl-formamide; Petroleum ether Ambient temperature;
参考文献
Lin, Ji-Mao; Liu, Ben-Sheng
Synthetic Communications, 1997 , vol. 27, # 5 p. 739 - 749
反应条件
molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran T=20°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 8 p. 2498 - 2503
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide Ambient temperature;
参考文献
Dedier, James; Gerval, Pierre; Frainnet, Emile
Journal of Organometallic Chemistry, 1980 , vol. 185, # 2 p. 183 - 198
反应条件
triethylamine in diethyl ether 1 h; Ambient temperature;
参考文献
Emde, Herbert; Goetz, Andreas; Hofmann, Karin; Simchen, Gerhard
Liebigs Annalen der Chemie, 1981 , # 9 p. 1643 - 1657
反应条件
triethylamine in N,N-dimethyl-formamide
参考文献
Synthesis, , p. 196 - 197
反应条件
carbon monoxide in n-heptane Kinetics; Addn. of Me2CHCHO to soln. of Co complex (n-heptane, CO, 25°C), stirring (1 h) until gas evolution ceased, color change from light brown to dark, further products.; GC-MS;
参考文献
Organometallics, , vol. 7, p. 1025 - 1028
反应条件
zinc(II) chloride in ethyl acetate 3 h; Ambient temperature;
参考文献
Makin, S. M.; Kruglikova, R. I.; Popova, T. P.; Tagirov, T. K.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 630 - 634
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 723 - 727
反应条件
potassium tert-butylate 1) THF, -50 deg C, 45 min; 2) THF, -50 deg C, 15 min; Yield given. Multistep reaction;
参考文献
Duhamel, Pierre; Cahard, Dominique; Poirier, Jean-Marie
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2509 - 2512
反应条件
BnNMe3(+)F(-) in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
反应条件
BnNMe3(+)F(-) in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Hirsch, Elisabeth; Huenig, Siegfried; Reissig, Hans-Ulrich
Chemische Berichte, 1982 , vol. 115, # 12 p. 3687 - 3696
