1,3-二甲基-6-氨基脲嘧啶合成路线 (共 109 条)
反应条件
1: With acetic anhydride T=60°C; 0.166667 h; microwave irradiation; 2: With sodium hydroxide in ethanol T=20°C;
参考文献
Devi, Ipsita; Bhuyan, Pulak J.
Tetrahedron Letters, 2005 , vol. 46, # 34 p. 5727 - 5729
反应条件
in 1,2,3,4-tetrahydro-naphthalene T=150°C; 0.0833333 h;
参考文献
Hirota, Kosaku; Maruhashi, Kazuo; Asao, Tetsuji; Senda, Shigeo
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 9 p. 3377 - 3379
反应条件
piperidine in ethanol T=20°C; 1 h;
参考文献
Deb, Mohit L.; Majumder, Swarup; Bhuyan, Pulak J.
Synlett, 2009 , # 12 p. 1982 - 1984
反应条件
diethylamine; acetophenone T=100 - 110°C; 3 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 2 p. 191 - 200
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 2 p. 224 - 233
反应条件
sodium methylate in methanol 5 h; Heating;
参考文献
Shorshnev, S. V.; Esipov, S. E.; Chernyshev, A. I.; Pozharskii, A. F.; Kuz'menko, V. V.; Gulevskaya, A. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1990 , vol. 26, # 2 p. 191 - 200
Khimiya Geterotsiklicheskikh Soedinenii, 1990 , vol. 26, # 2 p. 224 - 233
反应条件
chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane Cyclization; 24 h; Heating;
参考文献
Fuelle, Friederike; Mueller, Christa E.
Heterocycles, 2000 , vol. 53, # 2 p. 347 - 351
反应条件
acetic acid; trifluoroacetic acid 6 h; Heating;
参考文献
Khattab; Kappe
Monatshefte fur Chemie, 1996 , vol. 127, # 8-9 p. 917 - 925
参考文献
Saikia, Binoy K.; Das, Subrata; Sridhar, Balasubramaniam; Thakur, Ashim J.
Journal of Chemical Crystallography, 2012 , vol. 42, # 7 p. 711 - 720
反应条件
sodium amide; xylene T=100 - 120°C;
参考文献
DE165561 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 8, p. 1140
反应条件
diethylamine T=100 - 110°C; 3 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 26, # 2 p. 191 - 200
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 26, # 2 p. 224 - 233