1-碘-4-[2-(4-碘苯基)乙基]苯合成路线 （共 7 条）
参考文献
Elbs; Jaroslawzew
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 92
反应条件
methyl iodide
T=120°C;
参考文献
Tour, James M.; Rawlett, Adam M.; Kozaki, Masatoshi; Yao, Yuxing; Jagessar, Raymond C.; Dirk, Shawn M.; Price, David W.; Reed, Mark A.; Zhou, Chong-Wu; Chen, Jia; Wang, Wenyong; Campbell, Ian
Chemistry - A European Journal, 2001 , vol. 7, # 23 p. 5118 - 5134
反应条件
sodium tetrahydroborate; C69H94CoN8O20P in isopropyl alcohol
T=90°C; 0.25 h; Microwave irradiation;
参考文献
Giedyk; Fedosov; Gryko
Chemical Communications, 2014 , vol. 50, # 36 p. 4674 - 4676
反应条件
1.1: 59 percent / hydrogen / Pd/C / ethanol / 5 h / 20 °C / 3102.97 Torr
2.1: sodium nitrite; hydrochloric acid / H2O / 0.5 h / 0 °C
2.2: 87 percent / potassium carbonate / H2O
3.1: 78 percent / MeI / 120 °C
View Scheme
参考文献
Tour, James M.; Rawlett, Adam M.; Kozaki, Masatoshi; Yao, Yuxing; Jagessar, Raymond C.; Dirk, Shawn M.; Price, David W.; Reed, Mark A.; Zhou, Chong-Wu; Chen, Jia; Wang, Wenyong; Campbell, Ian
Chemistry - A European Journal, 2001 , vol. 7, # 23 p. 5118 - 5134
反应条件
sodium peroxodisulphate; iodine; acetic acid
参考文献
Elbs; Jaroslawzew
Journal fuer Praktische Chemie (Leipzig), 1913 , vol. <2> 88, p. 92
反应条件
1.1: sodium nitrite; hydrochloric acid / H2O / 0.5 h / 0 °C
1.2: 87 percent / potassium carbonate / H2O
2.1: 78 percent / MeI / 120 °C
View Scheme
参考文献
Tour, James M.; Rawlett, Adam M.; Kozaki, Masatoshi; Yao, Yuxing; Jagessar, Raymond C.; Dirk, Shawn M.; Price, David W.; Reed, Mark A.; Zhou, Chong-Wu; Chen, Jia; Wang, Wenyong; Campbell, Ian
Chemistry - A European Journal, 2001 , vol. 7, # 23 p. 5118 - 5134
反应条件
di-tert-butyl peroxide
参考文献
Johnston,K.M.J.; Williams,G.H.
Journal of the Chemical Society, 1960 , p. 1168 - 1171
