2-氯-2-氧-1,3,2-二氧磷杂环戊烷合成路线 （共 26 条）
反应条件
triethylamine 1.) benzene, RT, 4 h, 2.) CH3CN, 65 deg C; Yield given. Multistep reaction;
参考文献
Marx; Piantadosi; Noseda; Daniel; Modest
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 858 - 863
反应条件
triethylamine in dichloromethane T=0°C; Rate constantKinetics;
参考文献
Corriu, R. J. P.; Lanneau, G. F.; Leclercq, D.
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 18, p. 197 - 200
反应条件
diisopropylamine in tetrahydrofuran T=0 - 20°C; 2 h;
参考文献
Campins, Nathalie; Dieudonne, Philippe; Grinstaff, Mark W.; Barthelemy, Philippe
New Journal of Chemistry, 2007 , vol. 31, # 11 p. 1928 - 1934
反应条件
2,6-dimethylpyridine in benzene T=20°C; Cooling with ice;
参考文献
Iwasaki, Yasuhiko; Kawakita, Takashi; Yusa, Shin-Ichi
Chemistry Letters, 2009 , vol. 38, # 11 p. 1054 - 1055
反应条件
triethylamine 1.) benzene, RT, 4 h, 2.) CH3CN, 65 deg C; Yield given. Multistep reaction;
参考文献
Marx; Piantadosi; Noseda; Daniel; Modest
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 858 - 863
反应条件
in tetrahydrofuran T=-20 - 20°C; 5.5 h; Inert atmosphere;
参考文献
BIOINTERACTIONS LIMITED, UNIVERSITY OF READING; SANDHU, Shivpal, S.; RAISIN-DADRE, Fanny; MCKENDRICK, John, Ennis; RHODES, Alan; ONIS, Simon, Jon
Patent: WO2012/175923 A1, 2012 ;
Location in patent: Page/Page column 17-18 ;
反应条件
triethylamine in benzene 50 h; Ambient temperature;
参考文献
Chandrakumar, Nizal S.; Hajdu, Joseph
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1197 - 1202
参考文献
Ilia, Gheorghe; Iliescu, Smaranda; Dehelean, Gheorghe; Popa, Adriana; Pacureanu, Liliana; Macarie, Lavinia; Pascariu, Aurelia
Phosphorus, Sulfur and Silicon and Related Elements, 2002 , vol. 177, # 8-9 p. 2049 - 2050
反应条件
triethylamine in benzene
参考文献
Modro, Tomasz A.; Graham, Douglas H.
Journal of Organic Chemistry, 1981 , vol. 46, # 9 p. 1923 - 1925
反应条件
trimethylamine in benzene
T=0°C; 0.5 h; Yield given;
参考文献
Menger; Peresypkin
Journal of the American Chemical Society, 2001 , vol. 123, # 23 p. 5614 - 5615
