2-氯-2-氧-1,3,2-二氧磷杂环戊烷合成路线 （共 26 条）
参考文献
Stenzel, Martina H.; Davis, Thomas P.
Australian Journal of Chemistry, 2003 , vol. 56, # 10 p. 1035 - 1038
参考文献
Leong, Kam; Jie, Wen; Zhuo, Ren-Xi; Mao, Hai-Quan
Patent: US2002/155092 A1, 2002 ;
反应条件
potassium hydroxide; silica gel; trichlorophosphate 1.) reflux; 2.) rt., 3 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 38, # 27 p. 4841 - 4844
反应条件
triethylamine in methanol; benzene
参考文献
Leong, Kam; Jie, Wen; Zhuo, Ren-Xi; Mao, Hai-Quan
Patent: US2002/155092 A1, 2002 ;
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=0 - 5°C; Substitution; 2 h;
参考文献
Lewis, Andrew L.; Stokes, Howard C. K.
Journal of Chemical Research - Part S, 1999 , # 10 p. 612 - 613
反应条件
water T=25°C; Kinetics;
参考文献
Koh, Han Joong; Kang, Suk Jin; Kevill, Dennis N.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 7 p. 1404 - 1415
参考文献
Tetrahedron Letters, , vol. 34, # 21 p. 3463 - 3466
反应条件
CCL (Yeast); triethylamine 1.) CHCl3, RT, 5 h, 2.) heptane, n-BuOH, RT, 20 h; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 21, # 17 p. 1763 - 1768
反应条件
in benzene T=60°C; Yield given;
参考文献
Kumar; Bhakuni
Tetrahedron Letters, 1993 , vol. 34, # 21 p. 3463 - 3466
反应条件
CCL (Yeast); triethylamine 1.) CHCl3, RT, 5 h, 2.) heptane, n-BuOH, RT, 20 h; Yield given. Multistep reaction;
参考文献
Kumar; Shanker
Synthetic Communications, 1991 , vol. 21, # 17 p. 1763 - 1768
