((E)-1,2-二溴乙烯基)-苯合成路线 (共 46 条)
反应条件
perchloric acid; dihydrogen peroxide; potassium bromide; ammonium molibdate in water
T=20°C; pH=1.0; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Conte, Valeria; Floris, Barbara; Galloni, Pierluca; Silvagni, Adriano
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 10 p. 1341 - 1344
反应条件
bromine in dichloromethane
T=20°C; 2 h; with and without graphite; further dibromoalkenes; MechanismProduct distribution;
参考文献
Kodomari; Sakamoto; Yoshitomi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 4053 - 4054
反应条件
bis(dimethylacetamide)hydrogen tribromide in chloroform
T=-10°C; other unsaturated compounds, other brominating agent, var. temp.; cis- vs. trans ratios; Product distribution;
参考文献
Rodygin, M. Yu.; Mikhailov, V. A.; Zubritskii, M. Yu.; Savelova, V. A.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 3.1 p. 359 - 363
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 3 p. 339 - 343
反应条件
bromine; tin(IV) chloride in tetrachloromethane
Heating; Further byproducts. Title compound not separated from byproducts.;
参考文献
Martynov; Amosova; Makhaeva
Russian Journal of General Chemistry, 2005 , vol. 75, # 11 p. 1840 - 1841
反应条件
in dichloromethane
T=-5 - 20°C; Cyclization; bromination; 1 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Mironov; Konovalov; Litvinov; Gubaidullin; Petrov; Shtyrlina; Zyablikova; Musin; Azancheev; Il'yasov
Russian Journal of General Chemistry, 1998 , vol. 68, # 9 p. 1414 - 1442
反应条件
bromine; acetic acid in tetrachloromethane
T=0°C; 0.5 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Manickam, Manickam C. Durai; Annalakshmi, Subramanian; Pitchumani, Kasi; Srinivasan, Chockalingam
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1008 - 1012
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=40 - 110°C; 24 h;
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 24 h;
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 24 h;
参考文献
Schuh, Kerstin; Glorius, Frank
Synthesis, 2007 , # 15 p. 2297 - 2306
反应条件
potassium hydroxide; hydrogen in water
参考文献
Funabiki, Takuzo; Hosomi, Hiroaki; Yoshida, Satohiro; Tarama, Kimio
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1560 - 1568