3-羟基吡啶-N-氧化物合成路线 (共 22 条)
反应条件
sodium perborate in acetic acid T=40°C;
参考文献
McKillop, Alexander; Kemp, Duncan
Tetrahedron, 1989 , vol. 45, # 11 p. 3299 - 3306
参考文献
Journal of the American Chemical Society, , vol. 71, p. 67,69
反应条件
in various solvent(s) T=28°C; 48 h; pseudomonas fluorescens PfE1 bacteria;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 29, # 6 p. 730 - 731
Khimiya Geterotsiklicheskikh Soedinenii, , # 6 p. 847 - 848
反应条件
water; hexachloride iridate(II) ion; Nitrous oxide Irradiation; Rate constant;
参考文献
Journal of Physical Chemistry, , vol. 84, # 5 p. 532 - 534
反应条件
bromine; sodium methylate 1.) 10percent aq. NaOH, 24 h; 2.) MeOH, DMF, RT, 1.5 h; Multistep reaction. Yields of byproduct given;
参考文献
Tiecco; Tingoli; Testaferri; et al.
Tetrahedron, 1986 , vol. 42, # 5 p. 1475 - 1485
反应条件
1: 65 percent 2: 85 percent / HNO3, NO2, H2SO4 View Scheme
参考文献
Swindell, Charles S.; Duffy, Ruth H.
Heterocycles, 1986 , vol. 24, # 12 p. 3373 - 3377
反应条件
triethylamine in acetonitrile T=100 - 110°C; Substitution; 8 h;
参考文献
Leroy; Bigan; Blondeau
Synthetic Communications, 1997 , vol. 27, # 17 p. 2905 - 2916
反应条件
1: triethylamine, chlorotrimethylsilane / dimethylformamide / 12 h / 100 - 110 °C 2: methanol View Scheme
参考文献
Vorbrueggen, Helmut; Krolikiewicz, Konrad
Synthesis, 1983 , # 4 p. 316 - 319
反应条件
N,N-dimethylcarbamoyl chloride in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Fife, Wilmer K.
Heterocycles, 1984 , vol. 22, # 1 p. 93 - 96
反应条件
in dichloromethane Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Fife, Wilmer K.
Heterocycles, 1984 , vol. 22, # 1 p. 93 - 96