苯并(h)喹啉-5,6-二酮合成路线 （共 15 条）
反应条件
sodium hydroxide T=80 - 85°C; 0.5 h;
参考文献
Braven, J.; Hanson, R. W.; Smith, N. G.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 1051 - 1056
反应条件
1: 4 percent / 10percent aq. NaOH / 0.5 h / 80 - 85 °C 2: 85 percent / NaBH4 / propan-2-ol; tetrahydrofuran / 2.5 h / 60 - 70 °C View Scheme
参考文献
Braven, J.; Hanson, R. W.; Smith, N. G.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 1051 - 1056
反应条件
in acetonitrile T=24.84°C; reduction; oxidation; Irradiation; KineticsQuantum yield; Further Variations:Reaction partners;
参考文献
Fukuzumi, Shunichi; Itoh, Shinobu; Komori, Takashi; Suenobu, Tomoyoshi; Ishida, Akito; Fujitsuka, Mamoru; Ito, Osamu
Journal of the American Chemical Society, 2000 , vol. 122, # 35 p. 8435 - 8443
反应条件
in acetonitrile T=24.84°C; reduction; oxidation; Irradiation; KineticsQuantum yield;
参考文献
Journal of the American Chemical Society, , vol. 122, # 35 p. 8435 - 8443
反应条件
1: With acetic acid
T=108°C; 2 h;
2: With water; sodium hydrogencarbonate in chloroform
参考文献
CANON KABUSHIKI KAISHA
Patent: US2008/154040 A1, 2008 ;
Location in patent: Page/Page column 27 ;
反应条件
diiodine pentaoxide; acetic acid
2 h; Heating;
参考文献
Braven, J.; Hanson, R. W.; Smith, N. G.
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 1051 - 1056
反应条件
chromium(VI) oxide; water; silica gel; lithium diisopropyl amide
1) THF, 0 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Brandao, Marcos A. F.; Oliveira, Alaide Braga de; Snieckus, Victor
Tetrahedron Letters, 1993 , vol. 34, # 15 p. 2437 - 2440
反应条件
1: nitrobenzene; concentrated sulfuric acid / 150 - 160 °C
2: chromic acid; glacial acetic acid
View Scheme
参考文献
Skraup; Cobenzl
Monatshefte fuer Chemie, 1883 , vol. 4, p. 456
参考文献
Mustafa et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3409,3412
参考文献
Mustafa et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3409,3412
