(E)-3-硝基肉桂酸甲酯合成路线 (共 15 条)
反应条件
hydrogen; palladium on activated charcoal in methanol; benzene T=25°C; 24 h;
参考文献
Suzuki, Masaaki; Koyano, Hiroshi; Noyori, Ryoji; Hashimoto, Hitoshi; Negishi, Manabu; Ichikawa, Atsushi; Ito, Seiji
Tetrahedron, 1992 , vol. 48, # 13 p. 2635 - 2658
反应条件
trifluoroacetic acid; palladium diacetate in acetone
T=70°C; oxidative Heck reaction; 20 h;
参考文献
Ruan, Jiwu; Li, Xinming; Saidi, Ourida; Xiao, Jianliang
Journal of the American Chemical Society, 2008 , vol. 130, # 8 p. 2424 - 2425
反应条件
sodium methylate in N,N-dimethyl-formamide
参考文献
Curis, Inc.; Bao, Rudi; Lai, Chengjung; Qian, Changgeng
Patent: US2013/102595 A1, 2013 ;
Location in patent: Paragraph 0623; 0624 ;
反应条件
palladium diacetate in water
T=20°C; Heck type reaction; 0.5 h; solid phase reaction;
参考文献
Zarei, Amin; Khazdooz, Leila; Pirisedigh, Azadeh; Hajipour, Abdol R.; Seyedjamali, Hojjat; Aghaei, Hamidreza
Tetrahedron Letters, 2011 , vol. 52, # 35 p. 4554 - 4557
反应条件
tert.-butylnitrite; methanesulfonic acid; palladium diacetate in methanol
T=25°C; Heck Reaction; 48 h; Reagent/catalyst;
参考文献
Oger, Nicolas; Le Callonnec, Francois; Jacquemin, Denis; Fouquet, Eric; Le Grognec, Erwan; Felpin, Francois-Xavier
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 5 p. 1065 - 1071
反应条件
sulfuric acid in methanol; water
参考文献
Microcide Pharmaceuticals, Inc.; DAIICHI PHARMACEUTICAL CO., LTD.
Patent: EP1227084 A1, 2002 ;
反应条件
BuTeBu in tetrahydrofuran
6 h; Heating;
参考文献
Huang, Xian; Xie, Linghong; Wu, Hong
Tetrahedron Letters, 1987 , vol. 28, # 7 p. 801 - 802
反应条件
sulfuric acid
Esterification; 0.0833333 h; Irradiation;
参考文献
Mitra; De; Karchaudhuri
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 4 p. 311 - 312
参考文献
Watkins, Clare; Romero-Martin, Maria Rosario; Moore, Kathryn G; Ritchie, James; Finn, Paul W; Kalvinsh, Ivars; Loza, Einars; Dikovska, Klara; Gailite, Vija; Vorona, Maxim; Piskunova, Irina; Starchenkov, Igor; Andrianov, Victor; Harris, C. John; Duffy, James E.S.
Patent: US2004/77726 A1, 2004 ;
反应条件
potassium dihydrogenphosphate; 5 Pd(II)/C(eggshell) in ethanol; water
Heck reaction; 2 h; Reflux;
参考文献
Yuan, Yan-Qin; Guo, Sheng-Rong
Synthetic Communications, 2012 , vol. 42, # 7 p. 1059 - 1069