2-氯-5-(三氟甲基)苯甲酰氯合成路线 （共 6 条）
反应条件
thionyl chloride Heating;
参考文献
Helvetica Chimica Acta, , vol. 45, p. 2226 - 2241
反应条件
N,N-dimethyl-formamide in dichloromethane
参考文献
US2003/55085 A1, ;
US 20030055085 A1
反应条件
1.1: n-BuLi; tetramethylethylenediamine / diethyl ether; hexane / 0.33 h / -100 °C 1.2: 88 percent / diethyl ether; hexane / 2 h / -100 °C 2.1: SOCl2 / dimethylformamide / 12 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 36, # 3 p. 287 - 300
反应条件
1.1: Br2; SbCl5; Cl2 2.1: n-BuLi; tetramethylethylenediamine / diethyl ether; hexane / 0.33 h / -100 °C 2.2: 88 percent / diethyl ether; hexane / 2 h / -100 °C 3.1: SOCl2 / dimethylformamide / 12 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds, , vol. 36, # 3 p. 287 - 300
反应条件
1: aq. NaOH / Heating 2: SOCl2 / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 45, p. 2226 - 2241
反应条件
1: (i) NaNO2, H2SO4, (ii) aq. ZnCl2, (iii) /BRN= 3587243/, CuCN, aq. NaHCO3, PE 2: aq. NaOH / Heating 3: SOCl2 / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 45, p. 2226 - 2241
