in hexane
anhydrous and oxygen-free condns., BCl3 condensed into a stirred soln. of B-compd. in hexane at 0°C, cooled with an ice bath, allowed to attain ambient temp. within 30 min, stirred for 1 h; removal of volatile compds. in vac. (ClB(NMe2)2), distn.; elem. anal.;
Kyker,G.S.; Schram,E.P.
Journal of the American Chemical Society, 1968 , vol. 90, p. 3672 - 3677
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Gmelin Handbook: B: B-Verb.3, 10.4.4.1, page 174 - 175
Kyker,G.S.; Schram,E.P.
Journal of the American Chemical Society, 1968 , vol. 90, p. 3672 - 3677
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Gmelin Handbook: B: B-Verb.4, 2.4, page 32 - 40
