2-(6-溴己基)-丙二酸二乙酯合成路线 （共 16 条）
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
water; Marlonreg; AS3-acid T=150°C; 3 - 4 h; Neat (no solvent);
参考文献
Degussa AG
Patent: EP1384706 A1, 2004 ;
Location in patent: Page/Page column 6 ;
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C 2: 76 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h 3: H2 / PtO2 / diethyl ether View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C 2: NH3 / tetrahydrofuran / 15 h 3: diethyl ether 4: LiAlH4 / diethyl ether / 2 h / 0 °C View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C 2: 76 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h 3: H2 / PtO2 / diethyl ether 4: pyridine / 0 °C 5: NaI / acetone / 2 h / Heating View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C 2: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h 3: H2 / PtO2 / diethyl ether View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: 48percent HBr / H2O / 4 h / 120 - 150 °C 2: 58 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h 3: H2 / PtO2 / diethyl ether View Scheme
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
反应条件
1: aqueous hydrobromic acid View Scheme
参考文献
Salmon-Legagneur; Neveu
Bulletin de la Societe Chimique de France, 1956 , p. 1345,1350
反应条件
polyethyleneglycol monomethylether; potassium carbonate; tetrabutylammomium bromide in cyclohexane
参考文献
Degussa AG
Patent: EP1384706 A1, 2004 ;
Location in patent: Page/Page column 5 ;
反应条件
sodium ethanolate in diethyl ether; ethanol
48 h; Ambient temperature;
参考文献
Riche, Francoise; Mathieu, Jean-Paul; Vincens, Maurice; Bardy, Andre; Comet, Michel; Vidal, Michel
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 1-2 p. 49 - 55
