4-甲氧基-beta-甲基-氢化肉桂酸甲酯合成路线 （共 4 条）
反应条件
tert-butyl-amphos chloride; sodium lauryl sulfate; sodium carbonate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in toluene
T=80°C;
参考文献
Lautens, Mark; Mancuso, John; Grover, Harpreet
Synthesis, 2004 , # 12 p. 2006 - 2014
反应条件
hydrogen; palladium on activated charcoal in methanol
5 h;
参考文献
Tori, Motoo; Sono, Masakazu; Nishigaki, Yukiko; Nakashima, Katsuyuki; Asakawa, Yoshinori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 435 - 445
反应条件
1: 1.) NaH / 1.) benzene, rt, 1 h 2.) benzene, reflux, 7 h
2: 5 g / H2 / 10percent Pd-C / methanol / 5 h
View Scheme
参考文献
Tori, Motoo; Sono, Masakazu; Nishigaki, Yukiko; Nakashima, Katsuyuki; Asakawa, Yoshinori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 2 p. 435 - 445
反应条件
(i), (ii) (dehydration), (iii) (hydrogenation); Multistep reaction;
参考文献
Howe,I. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1969 , p. 439 - 445
