6-氯吡啶-2-硼酸频哪酯合成路线 （共 2 条）
反应条件
1: 2-Bromo-6-chloropyridine With n-butyllithium in tetrahydrofuran T=-78°C; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; 3: 2,3-dimethylbutane-2,3-diol With acetic acid in tetrahydrofuran
参考文献
Bouillon, Alexandre; Lancelot, Jean-Charles; Santos, Jana Sopkova De Oliveira; Collot, Valerie; Bovy, Philipppe R.; Rault, Sylvain
Tetrahedron, 2003 , vol. 59, # 50 p. 10043 - 10049
反应条件
1.1: nBuLi / tetrahydrofuran / -78 °C 1.2: 67 percent / C2Cl6 / tetrahydrofuran / -78 - 20 °C 2.1: nBuLi / tetrahydrofuran / -78 °C 2.2: B(OiPr)3 / tetrahydrofuran / -78 - 20 °C 2.3: 38 percent / glacial acetic acid / tetrahydrofuran View Scheme
参考文献
Tetrahedron, , vol. 59, # 50 p. 10043 - 10049
