2-甲基-6,7-二甲氧基-1,2,3,4-四氢异喹啉-1-酮合成路线 （共 61 条）
反应条件
1: 5 percent / methionine; methanesulphonic acid / neat (no solvent) 2: lithium aluminium hydride / tetrahydrofuran View Scheme
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=20°C; 1.5 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=20°C; 1.5 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=20°C; 1.5 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in water; acetonitrile
T=20°C; 1.5 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
oxygen in methanol
Oxidation; 1 h;
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Kanbayashi, Ryo; Tokuda, Masao; Suginome, Hiroshi
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6583 - 6596
反应条件
sodium hydride in benzene
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
反应条件
iodosylbenzene; tetra-(n-butyl)ammonium iodide in water; acetonitrile
1 h;
参考文献
Huang, Wei-Jan; Singh, Om V.; Chen, Chung-Hsiung; Chiou, Sheng-You; Lee, Shoei-Sheng
Helvetica Chimica Acta, 2002 , vol. 85, # 4 p. 1069 - 1078
反应条件
potassium tert-butylate
8 h; Heating;
参考文献
Blasko, Gabor; Hussain, S. Fazal; Shamma, Maurice
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1599 - 1602
反应条件
potassium tert-butylate
8 h; Heating;
参考文献
Blasko, Gabor; Hussain, S. Fazal; Shamma, Maurice
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1599 - 1602
