3-邻枯烯基-2-甲基丙醛合成路线 （共 3 条）
反应条件
1: With oxygen; sodium acetate; acetylacetone; palladium diacetate in propionic acid
T=90°C; P=760.051 Torr; 1.5 h;
2: With hydrogen; palladium on activated charcoal
P=760.051 Torr; Further stages. Title compound not separated from byproducts.;
参考文献
Yamada, Tomoyuki; Sakaguchi, Satoshi; Ishii, Yasutaka
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5471 - 5474
反应条件
hydrogen; potassium carbonate; palladium/alumina in ethanol
T=60°C; P=15200 Torr; var. pressure, var. temp., var. composition of catalysts, without K2CO3; Product distribution;
参考文献
Pak, A. M.; Ginzburg, M. A.; Turganbaeva, S. M.; Gabdrakipov, V. Z.; Kartonozhkina, O. I.; et al.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 6 p. 1040 - 1043
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 6 p. 1176 - 1180
反应条件
hydrogen; sodium carbonate; Catalyst M-Chromium oxide; nickel in ethanol; water
T=110°C; P=22800 Torr; other temperature, other solvent, other pressure, other catalysts; Product distribution;
参考文献
Sokol'skii, D. V.; Pak, A. M.; Turganbaeva, S. M.; Konuspaev, S. R.; Ginzburg, M. A.
J. Appl. Chem. USSR (Engl. Transl.), 1981 , vol. 54, # 7 p. 1574 - 1578,1345 - 1347
