in chloroform addn. of Sb-compd. to suspn. of chloroacetate, refluxing (24 h, pptn.); sepn. of ppt., filtration, distn. of solvent, recrystn. (petroleum ether); elem. anal.;
参考文献
Singh Raizada, Meenu; Srivastava
Journal of the Indian Chemical Society, 1996 , vol. 73, # 12 p. 646 - 649
in ethylene glycol dimethyl ether 22 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Busby, Reginald E.; Khan, Mohammad A.; Khan, Mohammad R.; Parrick, John; Shaw, C. J. Granville; Iqbal, Mohammad
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1427 - 1430