3-环己烯-1-羧酸甲酯合成路线 (共 53 条)
反应条件
hydrogen; sodium methylate; C44H48Cl2N2P2Ru in tetrahydrofuran T=80 - 100°C; P=37503.8 Torr; 2.5 - 5 h; Autoclave; Product distribution / selectivity;
参考文献
SAUDAN, Lionel; Dupau, Philippe; Riedhauser, Jean-Jacques; Wyss, Patrick
Patent: US2008/71098 A1, 2008 ;
Location in patent: Page/Page column 9 ;
反应条件
hydrogen; sodium methylate; C44H48Cl2N2P2Ru in tetrahydrofuran T=100°C; P=37503.8 Torr; 2.5 h; Autoclave; Product distribution / selectivity;
参考文献
SAUDAN, Lionel; Dupau, Philippe; Riedhauser, Jean-Jacques; Wyss, Patrick
Patent: US2008/71098 A1, 2008 ;
Location in patent: Page/Page column 9 ;
反应条件
InI3; dimethylphenylsilane in dichloromethane T=20°C; 1.66667 h; Inert atmosphere; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 18 p. 3382 - 3386