(9CI)-4-(苯基甲基)-嘧啶合成路线 （共 10 条）
反应条件
1: 60 percent / 70percent m-chloroperbenzoic acid / benzene / 18 h / Ambient temperature 2: 45 percent / 800 °C / 0 - 0 Torr View Scheme
参考文献
Ohsawa, Akio; Kawaguchi, Takayuki; Igeta, Hiroshi
Synthesis, 1983 , # 12 p. 1037 - 1040
反应条件
magnesium oxide; palladium on activated charcoal in ethanol; water
P=760 Torr; Ambient temperature;
参考文献
Abbotto, Alessandro; Alanzo, Vito; Bradamante, Silvia; Pagani, Giorgio A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 481 - 488
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=50°C; Negishi cross-coupling reaction; Inert atmosphere;
参考文献
Blachut, Dariusz; Szawkalo, Joanna; Czarnocki, Zbigniew
Synthesis, 2011 , # 21 art. no. T60411SS, p. 3496 - 3506
反应条件
hydrogen bromide
T=110°C; 1.5 h;
参考文献
Abbotto, Alessandro; Alanzo, Vito; Bradamante, Silvia; Pagani, Giorgio A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 481 - 488
反应条件
2: 76 percent / MgO / 10percent Pd/C / ethanol; H2O / 760 Torr / Ambient temperature
View Scheme
参考文献
Abbotto, Alessandro; Alanzo, Vito; Bradamante, Silvia; Pagani, Giorgio A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 481 - 488
反应条件
1: 1) NaNH2 / 1) THF, 15 min, RT, 2) THF, 1 h, RT
2: 71 percent / H2, MgO / 10percent Pd/C / ethanol; H2O / 760 Torr / Ambient temperature
3: 54 percent / 48percent hydrobromic acid / 1.5 h / 110 °C
View Scheme
参考文献
Abbotto, Alessandro; Alanzo, Vito; Bradamante, Silvia; Pagani, Giorgio A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 481 - 488
反应条件
1: 71 percent / H2, MgO / 10percent Pd/C / ethanol; H2O / 760 Torr / Ambient temperature
2: 54 percent / 48percent hydrobromic acid / 1.5 h / 110 °C
View Scheme
参考文献
Abbotto, Alessandro; Alanzo, Vito; Bradamante, Silvia; Pagani, Giorgio A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 481 - 488
反应条件
T=800°C; P=0.0001 - 0.0006 Torr;
参考文献
Ohsawa, Akio; Kawaguchi, Takayuki; Igeta, Hiroshi
Synthesis, 1983 , # 12 p. 1037 - 1040
反应条件
3-chloro-benzenecarboperoxoic acid in benzene
18 h; Ambient temperature;
参考文献
Ohsawa, Akio; Kawaguchi, Takayuki; Igeta, Hiroshi
Synthesis, 1983 , # 12 p. 1037 - 1040
反应条件
3-chloro-benzenecarboperoxoic acid in benzene
18 h; Ambient temperature;
参考文献
Ohsawa, Akio; Kawaguchi, Takayuki; Igeta, Hiroshi
Synthesis, 1983 , # 12 p. 1037 - 1040
