1,3-二甲基-2(1h)-吡啶酮合成路线 (共 9 条)
反应条件
1.) 145 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Gisby, Graham P.; Royall, Sven E.; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 169 - 174
反应条件
potassium carbonate in methanol
22 h; Reflux;
参考文献
Nakao, Yoshiaki; Idei, Hiroaki; Kanyiva, Kyalo Stephen; Hiyama, Tamejiro
Journal of the American Chemical Society, 2009 , vol. 131, # 44 p. 15996 - 15997
反应条件
und Behandeln des Reaktionsgemisches mit Kalium-hexacyanoferrat(III) und wss.Kalilauge;
参考文献
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286
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Bradlow; Vanderwerf
Journal of Organic Chemistry, 1951 , vol. 16, p. 73,79
反应条件
hydrogenchloride; potassium tert-butylate
n-butyl alcohol 1) 48h, reflux 2) cooled; Yield given. Multistep reaction;
参考文献
Coffen, David L.; Hengartner, Urs; Katonak, David A.; Mulligan, Mary E.; Burdick, David C.; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5109 - 5113
反应条件
potassium hydroxide
4 h; Heating;
参考文献
Buurman; Van der Plas
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1015 - 1018
反应条件
1: 80 percent / potassium permanganate, NH3(l) / 4 h / -33 °C
2: aq. KOH / 4 h / Heating
View Scheme
参考文献
Buurman; Van der Plas
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1015 - 1018
反应条件
acetic acid; platinum
Hydrogenation;
参考文献
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286
反应条件
1.) 145 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Gisby, Graham P.; Royall, Sven E.; Sammes, Peter G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 169 - 174
反应条件
1: platinum; acetic acid / Hydrogenation
2: sodium
View Scheme
参考文献
Leonard; Hauck
Journal of the American Chemical Society, 1957 , vol. 79, p. 5279,5286