1: (E)-2-phenyl-1-[tris(trimethylsilyl)germyl]ethene With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=20°C; 1 h; 2: iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=40°C; 15 h;
sodium acetate; lt;Pd(CH3CN)2Cl2gt;*6Ph4PCl in various solvent(s) T=140°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 37, # 4 p. 481 - 483
manganese; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=20°C; 18 h;
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Del Moral, Jose F. Quilez; Arteaga, Pilar; Akssira, Mohammed; El Hanbali, Fadwa; Arteaga, Jesus F.; Dieguez, Horacio R.; Sanchez, Elena M.
Journal of Organic Chemistry, 2007 , vol. 72, # 6 p. 2251 - 2254