in diethyl ether T=0 - 20°C; 20 h; Inert atmosphere;
参考文献
Duong, Hung A.; Gilligan, Ruth E.; Cooke, Michael L.; Phipps, Robert J.; Gaunt, Matthew J.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 463 - 466
1: With sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile in o-di-fluorobenzene T=75 - 80°C; 4 h; 2: With potassium hydroxide; potassium hydrogencarbonate; potassium iodide in o-di-fluorobenzene; water T=60°C; pH=6.3; Conversion of starting material;
