1: in acetone T=80°C; Diels-Alder reaction; 14 h; 2: With potassium tert-butylate in tetrahydrofuran 0.166667 h; Title compound not separated from byproducts;
参考文献
Bradley, Pamela J.; Grayson, David H.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 15 p. 1794 - 1799
1: benzenesulphinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide
T=20°C; 6 h; solid-phase reaction;
2: acrylonitrile With 2,2'-azo-bisisobutyronitrile in benzene
20 h; Heating;
3: With dihydrogen peroxide in tetrahydrofuran
T=20°C; 2 h;
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 1025 - 1029
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , # 6 p. 1075 - 1080
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1966 , p. 1025 - 1029
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1966 , # 6 p. 1075 - 1080
