5-甲基-2-硝基苯甲腈合成路线 (共 21 条)
反应条件
trichlorophosphate in DMF (N,N-dimethyl-formamide) T=-10 - 100°C; 1.25 h;
参考文献
Xiao, Zejun; Kochat, Harry
Patent: US2004/92739 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
pyridinium chlorochromate in chloroform 3 h; Reflux;
参考文献
Chandrappa; Prasanna; Vinaya; Rangappa
Synthetic Communications, 2013 , vol. 43, # 20 p. 2756 - 2762
反应条件
sulfuric acid; potassium nitrate
参考文献
Chemische Berichte, , vol. 38, p. 3555
反应条件
in various solvent(s) T=160°C; 5 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 2 p. 345 - 349
反应条件
N-bromosuccinmide 1.) MeCN, 10 min, 2.) MeCN, 30 min; Yield given. Multistep reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 503, # 2 p. 171 - 184
反应条件
1: 1.) SOCl2; 2.) NH4OH / 1.) PhMe, reflux 2: SOCl2 / Heating View Scheme
参考文献
Tetrahedron, , vol. 50, # 18 p. 5515 - 5525
反应条件
nitrogen(IV) oxide; ozone in acetonitrile T=-10°C; Kyodai nitration; 3 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 13 p. 2326 - 2335
反应条件
hydrogenchloride; water; sodium nitrite
参考文献
Chemische Berichte, , vol. 31, p. 394
参考文献
Bull. Sect. Sci. Acad. Roum., , vol. 28, p. 354,359
反应条件
hydrogenchloride T=150°C; im geschlossenen Rohr;
参考文献
Findeklee
Chemische Berichte, 1905 , vol. 38, p. 3555