1,2-二溴-3,3-二甲基丁烷合成路线 (共 13 条)
反应条件
18-crown-6 ether; potassium tert-butylate in Petroleum ether T=60°C; 2 h;
参考文献
Dehmlow, Eckehard V.; Lissel, Manfred
Liebigs Annalen der Chemie, 1980 , # 1 p. 1 - 13
反应条件
potassium hydroxide; Aliquatreg; 336 in xylene Heating;
参考文献
Zakrzewski; Huras; Sas; Zelechowski; Bombinska
Polish Journal of Chemistry, 2008 , vol. 82, # 5 p. 1051 - 1057
反应条件
potassium hydroxide; Aliquatreg; 336 in xylene Heating;
参考文献
Zakrzewski; Huras; Sas; Zelechowski; Bombinska
Polish Journal of Chemistry, 2008 , vol. 82, # 5 p. 1051 - 1057
反应条件
sodium methylate in dichloromethane 24 h; Heating; Title compound not separated from byproducts;
参考文献
Sydnes, Leiv K.; Alnes, Karl F. S.; Erdogan, Natalia
Monatshefte fur Chemie, 2005 , vol. 136, # 10 p. 1737 - 1749
反应条件
bromine
0.133333 h; Phase-vanishing reaction with phase screenNeat (no solvent)Darkness;
参考文献
Pels, Kevin; Dragojlovic, Veljko
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. A75
参考文献
Collier,W.L.; Macomber,R.S.
Journal of Organic Chemistry, 1973 , vol. 38, p. 1367 - 1369
反应条件
in dichloromethane; benzene
T=14 - 15°C; Irradiation;
参考文献
Tlumak, Robert L.; Skell Philip S.
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7267 - 7274
反应条件
bromine
unter Lichtausschluss;
参考文献
Puterbaugh; Newman
Journal of the American Chemical Society, 1957 , vol. 79, p. 3469
反应条件
bromine chloride in dichloromethane
T=0°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negoro, Takeshi; Ikeda, Yoshitsugu
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2547 - 2552
反应条件
in dichloromethane
T=17°C; Irradiation;
参考文献
Day, J. C.; Govindaraj, N.; McBain, D. S.; Skell, P. S.; Tanko, J. M.
Journal of Organic Chemistry, 1986 , vol. 51, # 25 p. 4959 - 4963