N-(2-氯苯基)-4-甲基苯磺酰胺合成路线 （共 15 条）
反应条件
in acetonitrile 4 h; Irradiation;
参考文献
Tetrahedron, , vol. 59, # 39 p. 7651 - 7659
反应条件
1: water; acetic acid; nitric acid 2: aqueous sulfuric acid View Scheme
参考文献
Holmes; Loudon
Journal of the Chemical Society, 1940 , p. 1521,1524
反应条件
1: water; acetic acid; nitric acid 2: aqueous sulfuric acid 3: sulfuric acid; sodium nitrite / Eintragen der Reaktionsloesung in eine wss. Loesung von Kalium-tetracyanoniccolat(II) und Natriumcarbonat View Scheme
参考文献
Holmes; Loudon
Journal of the Chemical Society, 1940 , p. 1521,1524
反应条件
in acetonitrile
4 h; Irradiation;
参考文献
Park, Kwanghee Koh; Lee, Jin Joo; Ryu, Jaegyung
Tetrahedron, 2003 , vol. 59, # 39 p. 7651 - 7659
反应条件
dipotassium peroxodisulfate; sodium chloride in water; acetonitrile
T=100°C; 2 h; regioselective reaction;
参考文献
Gu, Liuqun; Lu, Ting; Zhang, Mingyun; Tou, Lijuan; Zhang, Yugen
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1077 - 1082
反应条件
1: N-(2-chlorophenyl)-4-methyl-benzenesulfonamide With dichloro bis(acetonitrile) palladium(II); Cy-DHTP*HBF4; lithium tert-butylate in toluene
T=20°C; 0.666667 h; Inert atmosphere;
2: phenylacetylene in toluene
Sonogashira Cross-Coupling; 19 h; Inert atmosphereReflux;
参考文献
Yamaguchi, Miyuki; Manabe, Kei
Organic Letters, 2014 , vol. 16, # 9 p. 2386 - 2389
反应条件
(Na1752K0.144Ca0365Mg0.065)(Al2044Si2774O96)*19.16H2O in ethanol
T=25 - 30°C; 0.333333 h; SonicationGreen chemistry;
参考文献
Nasrollahzadeh, Mahmoud; Ehsani, Ali; Rostami-Vartouni, Akbar
Ultrasonics Sonochemistry, 2014 , vol. 21, # 1 p. 275 - 282
反应条件
1: para-thiocresol With thionyl chloride; dihydrogen peroxide in water; acetonitrile
T=25°C;
2: 2-chloro-aniline With pyridine in water; acetonitrile
T=25°C; 0.05 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Soheilizad, Mehdi
Journal of Organic Chemistry, 2009 , vol. 74, # 24 p. 9287 - 9291
反应条件
molecular sieve; tris(3,4,5-tribromopyrazol-1-yl)Cu(NCMe)
T=80°C;
参考文献
Fructos, Manuel R.; Trofimenko, Swiatoslaw; Mar Diaz-Requejo; Perez, Pedro J.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11784 - 11791
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide
T=135°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong
Synlett, 2011 , # 6 p. 837 - 843
