(E)-3-碘-2-丙酸合成路线 （共 25 条）
反应条件
sulfuric acid Esterification; 4 h; Heating;
参考文献
Takeuchi, Ryo; Tanabe, Keisuke; Tanaka, Shigeru
Journal of Organic Chemistry, 2000 , vol. 65, # 5 p. 1558 - 1561
反应条件
sulfuric acid Esterification; 4 h; Heating;
参考文献
Takeuchi, Ryo; Tanabe, Keisuke; Tanaka, Shigeru
Journal of Organic Chemistry, 2000 , vol. 65, # 5 p. 1558 - 1561
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide T=25°C; 3 h;
参考文献
Abarbri, Mohamed; Parrain, Jean-Luc; Cintrat, Jean-Christophe; Duchene, Alain
Synthesis, 1996 , # 1 p. 82 - 86
反应条件
hydrogen iodide in benzene Reflux;
参考文献
De Carne-Carnavalet, Benoit; Archambeau, Alexis; Meyer, Christophe; Cossy, Janin; Folleas, Benoit; Brayer, Jean-Louis; Demoute, Jean-Pierre
Organic Letters, 2011 , vol. 13, # 5 p. 956 - 959
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide T=25°C; 3 h;
参考文献
Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain
Synthetic Communications, 1998 , vol. 28, # 2 p. 239 - 249
反应条件
Multistep reaction.;
参考文献
Oates, Leslie J.; Jackson, Richard F.W.; Block, Michael H.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 1 p. 140 - 144
反应条件
1: trans-iodopropenoic acid With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Stille coupling; 0.25 h; Inert atmosphere; 2: dibutyldivinylstannane in N,N-dimethyl-formamide T=25°C; Stille coupling; 12 h; Inert atmosphere;
参考文献
Lamande-Langle, Sandrine; Abarbri, Mohamed; Thibonnet, Jerome; Duchene, Alain
Journal of Organometallic Chemistry, 2009 , vol. 694, # 15 p. 2368 - 2374
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide T=25°C; 3 h;
参考文献
Abarbri, Mohamed; Parrain, Jean-Luc; Cintrat, Jean-Christophe; Duchene, Alain
Synthesis, 1996 , # 1 p. 82 - 86
反应条件
1: trans-iodopropenoic acid With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Stille coupling; 0.25 h; Inert atmosphere; 2: tetravinyl tin in N,N-dimethyl-formamide T=30°C; Stille coupling; 12 h; Inert atmosphere;
参考文献
Lamande-Langle, Sandrine; Abarbri, Mohamed; Thibonnet, Jerome; Duchene, Alain
Journal of Organometallic Chemistry, 2009 , vol. 694, # 15 p. 2368 - 2374
反应条件
1: trans-iodopropenoic acid With bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Stille coupling; 0.25 h; Inert atmosphere; 2: n-butyltriphenylstannane in N,N-dimethyl-formamide T=60°C; Stille coupling; 12 h; Inert atmosphere;
参考文献
Lamande-Langle, Sandrine; Abarbri, Mohamed; Thibonnet, Jerome; Duchene, Alain
Journal of Organometallic Chemistry, 2009 , vol. 694, # 15 p. 2368 - 2374
