S-2-羟乙基-L-半胱氨酸合成路线 (共 13 条)
反应条件
sodium hydroxide 1.5 h; Ambient temperature;
参考文献
Larsson, Ulf; Carlson, Rolf
Acta Chemica Scandinavica, 1994 , vol. 48, # 6 p. 517 - 525
反应条件
potassium phosphate in water T=327°C; 24 h; enzyme catalyst: S-carboxymethyl-L-cysteine synthase from Escherichia coli W3110;
参考文献
Agricultural and Biological Chemistry, , vol. 53, # 9 p. 2481 - 2487
反应条件
sulfuric acid 4 h; Heating;
参考文献
Adams, Benjamin; Lowpetch, Kreingkrai; Thorndycroft, Faye; Whyte, Sheena M.; Young, Douglas W.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 18 p. 3357 - 3364
反应条件
triethylamine in ethanol
参考文献
Journal of Organic Chemistry, , vol. 28, p. 1105 - 1107
反应条件
sodium amide in ammonia
参考文献
Journal of Organic Chemistry, , vol. 29, p. 2203 - 2205
反应条件
1: C28H25Cl2N3NiO4 With acetic anhydride; sodium carbonate in acetonitrile T=25 - 70°C; 2: 2-hydroxyethanethiol With potassium carbonate in acetonitrile T=50°C; Michael condensation; 0.166667 h; 3: With hydrogenchloride; water in ethanol
参考文献
Tetrahedron Asymmetry, , vol. 21, # 21-22 p. 2638 - 2645
反应条件
1: C30H31N3NiO4 With acetic anhydride; sodium carbonate in acetonitrile T=25 - 70°C; 2: 2-hydroxyethanethiol With potassium carbonate in acetonitrile T=50°C; Michael condensation; 15 h; 3: With hydrogenchloride; water in ethanol
参考文献
Tetrahedron Asymmetry, , vol. 21, # 21-22 p. 2638 - 2645
反应条件
1: C28H26ClN3NiO4 With acetic anhydride; sodium carbonate in acetonitrile T=25 - 70°C; 2: 2-hydroxyethanethiol With potassium carbonate in acetonitrile T=50°C; Michael condensation; 3 h; 3: With hydrogenchloride; water in ethanol
参考文献
Tetrahedron Asymmetry, , vol. 21, # 21-22 p. 2638 - 2645
反应条件
sodium hydrogencarbonate
参考文献
Journal of Pharmaceutical Sciences, , vol. 50, p. 312 - 315
反应条件
sodium hydrogencarbonate
参考文献
Biochemical Journal, , vol. 29, p. 1010