1,2,3,4-四氢喹啉合成路线 (共 372 条)
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 6 p. 481 - 485
反应条件
hydrogenchloride in water 24 h; Heating;
参考文献
Meyers, A. I.; Reuman, Michael; Gabel, Richard A.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 783 - 788
反应条件
1: With diisobutylaluminium hydride in hexane; dichloromethane T=0°C; 3.5 h; Inert atmosphere; 2: With NAF in hexane; dichloromethane; water T=0°C; 0.5 h; Inert atmosphere; regiospecific reaction;
参考文献
Cho, Hidetsura; Sugimoto, Kenji; Iwama, Yusuke; Mitsuhashi, Nakako; Okano, Kentaro; Tokuyama, Hidetoshi
Heterocycles, 2011 , vol. 82, # 2 p. 1633 - 1644
反应条件
palladium 10 on activated carbon; zinc in water; tert-butyl alcohol T=150°C; 40 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
1,4-dioxane; palladium T=50°C; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1927
反应条件
1,4-dioxane; palladium T=50°C; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 66, p. 1927
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether 1 h; Ambient temperature;
参考文献
Heterocycles, , vol. 14, # 1 p. 39 - 41
反应条件
in (R/S)-4-ethyl-1,2,3,4-tetrahydroquinoline
参考文献
US5688810 A1, ;
US 5688810 A
反应条件
hydrogenchloride; indium in water 5 h; Reflux;
参考文献
Heterocycles, , vol. 77, # 2 p. 1163 - 1170
反应条件
palladium 10 on activated carbon; zinc in water; isopropyl alcohol T=150°C; 40 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833