1,2,3,4-四氢喹啉合成路线 （共 372 条）
反应条件
boron trifluoride diethyl etherate; sodium cyanoborohydride in methanol 8 h; Heating;
参考文献
Srikrishna, Adusumilli; Reddy, T. Jagadeeswar; Viswajanani, Ranganathan
Tetrahedron, 1996 , vol. 52, # 5 p. 1631 - 1636
反应条件
hydrogen; nickel T=210°C; P=7600 Torr; or Ru/C, 100 atm, 150 deg C, and competitive hydrogenation with isoquinoline; Rate constant;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 11 p. 3167 - 3174
反应条件
diisobutylaluminium hydride in dichloromethane 1.) -78 deg C, 5 min, 2.) 0 deg C;
参考文献
Hattori, Kazunobu; Matsumura, Yasushi; Miyazaki, Tohru; Maruoka, Keiji; Yamamoto, Hisashi
Journal of the American Chemical Society, 1981 , vol. 103, # 24 p. 7368 - 7370
反应条件
1: With copper(l) iodide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene T=110°C; 23 h; 2: With acetic acid in tetrahydrofuran T=60°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 126, # 11 p. 3529 - 3533
反应条件
titanium(IV) isopropylate; chloro-trimethyl-silane; magnesium in tetrahydrofuran T=50°C; 12 h; Inert atmosphere;
参考文献
Shohji, Noriaki; Kawaji, Tsuyoshi; Okamoto, Sentaro
Organic Letters, 2011 , vol. 13, # 10 p. 2626 - 2629
反应条件
lithium triethylborohydride in tetrahydrofuran T=0°C; 1.5 h; Reagent/catalystSolventTimeTemperature;
参考文献
Nack, William A.; He, Gang; Zhang, Shu-Yu; Lu, Chengxi; Chen, Gong
Organic Letters, 2013 , vol. 15, # 13 p. 3440 - 3443
反应条件
2,6-dimethylpyridine; phenyl silane; In(OAc)3 in ethanol T=20°C; 19 h;
参考文献
Heterocycles, , vol. 80, # 1 p. 601 - 606
反应条件
C36H35IrN2P(1+)*C32H12BF24(1-); potassium tert-butylate in diethylene glycol dimethyl ether T=60°C; 24 h; Inert atmosphere;
参考文献
Li, Jia-Qi; Andersson, Pher G.
Chemical Communications, 2013 , vol. 49, # 55 p. 6131 - 6133
反应条件
quinoline in 1,4-dioxane T=175°C; 24 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 17 p. 5019 - 5021
反应条件
copper(l) iodide; caesium acetate in dimethyl sulfoxide T=20°C; 24 h;
参考文献
Yamada, Ken; Kubo, Tetsuji; Tokuyama, Hidetoshi; Fukuyama, Tohru
Synlett, 2002 , # 2 p. 231 - 234
