4-氨基苯甲酸甲酯盐酸盐合成路线 (共 10 条)
反应条件
[ReO2I(PPh3)2]; dimethylphenylsilane in toluene 1 h; Reflux; chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 18 p. 6960 - 6964
反应条件
thionyl chloride in methanol
参考文献
US4963539 A1, ;
US 4963539 A
反应条件
chloro-trimethyl-silane T=20°C; 24 h;
参考文献
Molecules, , vol. 13, # 5 p. 1111 - 1119
反应条件
thionyl chloride in methanol 3 h; Reflux;
参考文献
Research on Chemical Intermediates, , vol. 38, # 1 p. 77 - 89
反应条件
thionyl chloride in methanol 2 h; Reflux;
参考文献
Research on Chemical Intermediates, , vol. 38, # 1 p. 77 - 89
反应条件
in methanol T=75°C; 5 h;
参考文献
ChemMedChem, , vol. 9, # 3 p. 638 - 648
反应条件
1: potassium carbonate / acetone / 0 - 15 °C 2: thionyl chloride / methanol / 2 h / Reflux View Scheme
参考文献
Research on Chemical Intermediates, , vol. 38, # 1 p. 77 - 89
反应条件
1: 80 percent / glacial acetic acid / ethanol / 2 h / Heating 2: 80 percent / hydrazine hydrate / methanol / 16 h / Heating 3: 52 percent / glacial acetic acid / ethanol / 10 h / Heating View Scheme
参考文献
Singh, Inder Pal; Saxena, A. K.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 838 - 843
反应条件
1: 80 percent / glacial acetic acid / ethanol / 2 h / Heating 2: 80 percent / hydrazine hydrate / methanol / 16 h / Heating View Scheme
参考文献
Singh, Inder Pal; Saxena, A. K.; Shanker, K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 838 - 843
参考文献
Vanguard Medica Limited
Patent: US5877204 A1, 1999 ;