1,2,3-三甲氧基苯合成路线 （共 210 条）
反应条件
in chloroform Oxidation; 3 h; Heating; Further byproducts given;
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2001 - 2019
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 3 h; Ambient temperature;
参考文献
Matsumoto, Masakatsu; Kobayashi, Hisako; Hotta, Yasushi
Journal of Organic Chemistry, 1985 , vol. 50, # 10 p. 1766 - 1768
反应条件
potassium peroxymonosulfate in acetonitrile-D3; water-d2 T=20°C; 5 h; Solvent;
参考文献
Collom; Anastas; Beach; Crabtree; Hazari; Sommer
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2344 - 2347
反应条件
potassium peroxymonosulfate in acetonitrile-D3; water-d2; tert-butyl alcohol T=20°C; 5 h; Schlenk techniqueInert atmosphere;
参考文献
Collom; Anastas; Beach; Crabtree; Hazari; Sommer
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2344 - 2347
反应条件
in chloroform Oxidation; 3 h; Heating; Further byproducts given;
参考文献
Journal of Chemical Research, Miniprint, , # 8 p. 2001 - 2019
反应条件
lithium aluminium tetrahydride in benzene 6 h; Heating;
参考文献
Carrol, John F.; Kulkowit, Sunanta; McKervey, M. Anthony
Journal of the Chemical Society, Chemical Communications, 1980 , # 11 p. 507 - 508
反应条件
boron trichloride in dichloromethane 41 h; Ambient temperature;
参考文献
Australian Journal of Chemistry, , vol. 38, # 5 p. 777 - 792
反应条件
lithium chloride in N,N-dimethyl-formamide 48 h; Heating; Yield given. Yields of byproduct given;
参考文献
Bernard, Angela M.; Ghiani, M. Rossella; Piras, Pier Paolo; Rivoldini, Antonio
Synthesis, 1989 , # 4 p. 287 - 289
反应条件
1: 70 percent / Aluminium chloride / 1,2-dichloro-ethane / 2 h / 0 °C / 2.) Room temp., 3 h 2: 77 percent / Acetic acid, hydrogen chloride gas / 1.) Room temp., 2.) 60-70 deg C 3: 99 percent / acetonitrile / 1.5 h / Heating 4: 99 percent / Sodium borohydride / methanol; H2O / 1.) below 20 deg C, 2.) room temp., 1.5 h 5: 73 percent / Benzyltriethylammonium Permanganate / CH2Cl2 / 5 h / 20 °C 6: 61 percent / Aluminium chloride / 1,2-dichloro-ethane / 1.5 h / Heating 7: 71 percent / aniline / pyridine / 2 h / 60 °C 8: 72 percent / Copper powder, quinoline / 1 h / Heating View Scheme
参考文献
Nore; Honkanen
Journal of Heterocyclic Chemistry, 1980 , vol. 17, # 5 p. 985 - 987
反应条件
aluminium(III) iodide; tetra-(n-butyl)ammonium iodide in benzene 0.5 h; Heating;
参考文献
Andersson, Sven
Synthesis, 1985 , # 4 p. 437 - 439
