2-(4-氯苯基)-1-苯乙酮合成路线 (共 67 条)
反应条件
RhH(CO)(PPh3)3; bis(1,2-diphenylphosphino)benzene in 1,3-dimethyl-imidazolidin-2-one T=150°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 14 p. 3804 - 3807
反应条件
(i) NaOEt, EtOH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Imperial Chemical Industries, Ltd.
Patent: BE637389 , 1964 ;
Chem.Abstr., 1965 , vol. 62, # 10373
反应条件
sodium hydroxide; tetrabutylammomium bromide; palladium dichloride in water
T=130 - 160°C; 2 h; Microwave irradiation;
参考文献
Schmink, Jason R.; Leadbeater, Nicholas E.
Organic Letters, 2009 , vol. 11, # 12 p. 2575 - 2578
反应条件
sodium hydride in tetrahydrofuran
4 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Yang, Dongmei; Zhou, Yuhan; Xue, Na; Qu, Jingping
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4171 - 4176
反应条件
toluene-4-sulfonic acid in water; toluene
参考文献
Bayer Aktiengesellschaft
Patent: US4503059 A1, 1985 ;
反应条件
1: N2H4*H2O / Ambient temperature
2: CF3CO2Hg
View Scheme
参考文献
Theis,R.J.; Dessy,R.E.
Journal of Organic Chemistry, 1966 , vol. 31, p. 624 - 625
反应条件
T=20°C; unter Luftzutritt;
参考文献
Callow; Hill
Journal of the Chemical Society, 1937 , p. 844,847