4-氨基-N,N-二甲基苯甲酰胺合成路线 （共 16 条）
反应条件
1,1,3,3-tetramethyldisiloxane in ethanol T=20°C; 0.75 h; Inert atmosphereSonication; chemoselective reaction;
参考文献
Park, Sungho; Lee, In Su; Park, Jaiwook
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 3 p. 395 - 399
反应条件
1: With hydrogenchloride in 1,4-dioxane; dichloromethane T=20°C; 3 h; 2: With sodium carbonate in water pH=10;
参考文献
AC Immune, S.A.
Patent: US2011/280808 A1, 2011 ;
Location in patent: Page/Page column 52 ;
反应条件
1: in tetrahydrofuran T=20°C; 2 h; 2: With hydrogen; palladium on activated charcoal in methanol 3 h; Inert atmosphere;
参考文献
US2010/15141 A1, ;
Page/Page column 25-26 ;
US 20100015141 A1
反应条件
tert.-butylhydroperoxide; CuO in water T=80°C; 15 h;
参考文献
Priyadarshini; Amal Joseph; Lakshmi Kantam
RSC Advances, 2013 , vol. 3, # 40 p. 18283 - 18287
反应条件
1: aq. NaOH solution 2: tin (II)-chloride; aqueous hydrochloric acid; acetic acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 60, p. 1081
反应条件
1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol; EDC monohydrochloride / N,N-dimethyl-formamide / 12 h / 20 °C 2: methanol / palladium 10 on activated carbon / 3.17 h / 3102.97 Torr / Inert atmosphere View Scheme
反应条件
1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C 1.2: 20 °C 2.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C 2.2: pH 10 View Scheme
反应条件
1.1: sodium hydroxide / 1,4-dioxane; water / 20 °C 1.2: pH 3 2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C 2.2: 20 °C 3.1: hydrogenchloride / dichloromethane; 1,4-dioxane / 3 h / 20 °C 3.2: pH 10 View Scheme
参考文献
Journal of medicinal chemistry, , vol. 9, # 6 p. 892 - 911
反应条件
humic acid in water radical reaction; Irradiation;
参考文献
Pesticide Science, , vol. 46, # 2 p. 151 - 155
