2-(2-甲基苯氧基)苯甲酸合成路线 (共 11 条)
反应条件
copper(l) iodide; copper; potassium carbonate; pyridine in water
Ullmann-Goldberg condensation; 0.333333 h; ultrasound irradiation;
参考文献
Pellon Comdom, Rolando F.; Docampo Palacios, Maite L.
Synthetic Communications, 2003 , vol. 33, # 6 p. 921 - 926
反应条件
sodium hydroxide in methanol; water
Inert atmosphere;
参考文献
Wang, Congyang; Piel, Isabel; Glorius, Frank
Journal of the American Chemical Society, 2009 , vol. 131, p. 4194 - 4195
反应条件
methanol; sodium methylate; copper
参考文献
Cadogan; Hutchison; McNab
Tetrahedron, 1992 , vol. 48, # 36 p. 7747 - 7762
反应条件
in methanol; potassium carbonate
参考文献
Cancer Research Campaign Technology Limited
Patent: US5281620 A1, 1994 ;
反应条件
sodium methylate; copper diacetate
2.) 100 deg C, 5 h;
参考文献
Palmer; Rewcastle; Atwell; Baguley; Denny
Journal of Medicinal Chemistry, 1988 , vol. 31, # 4 p. 707 - 712
反应条件
tri[2-(2-methoxyethoxy)ethyl]amine; caesium carbonate; copper(l) chloride in 1,4-dioxane
Ullmann coupling; 20 h; Heating;
参考文献
Blake, Jessie A.; Gagnon, Eric; Lukeman, Matthew; Scaiano
Organic Letters, 2006 , vol. 8, # 6 p. 1057 - 1060
反应条件
pyridine; copper(l) iodide; copper; potassium carbonate
2 h; Heating;
参考文献
Pellon; Carrasco; Milian; Rodes
Synthetic Communications, 1995 , vol. 25, # 7 p. 1077 - 1083
反应条件
copper; ortho-cresol
T=200°C;
参考文献
Ullmann; Slokasow
Chemische Berichte, 1905 , vol. 38, p. 2115
Full Text Show Details
Akt.-Ges. f. Anilinf.
Patent: DE158998 ;
反应条件
[Rh(acac)(COD)]2; potassium iodide in acetic anhydride
T=160°C; 10 h; Inert atmosphere;
参考文献
Maetani, Shinji; Fukuyama, Takahide; Ryu, Ilhyong
Organic Letters, 2013 , vol. 15, # 11 p. 2754 - 2757
参考文献
Pickert, Martina; Frahm, August Wilhelm
Archiv der Pharmazie, 1998 , vol. 331, # 5 p. 177 - 192