3,4,5,6-四氯-1,2-苯二甲酸半水合物合成路线 （共 50 条）
反应条件
benzene
unter Entfernen des entstehenden Wassers;
参考文献
Teterin; Sonis
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 658,660
Chem. Zentralbl., 1936 , vol. 107, # II p. 2347
反应条件
1: glacial acetic acid / 300 °C
2: concentrated sulfuric acid; nitric acid
3: tin; fuming hydrochloric acid
View Scheme
参考文献
Tust
Chemische Berichte, 1887 , vol. 20, p. 2441
反应条件
1: acetic acid / beim Erhitzen auf Siedetemperatur
2: lithium alanate; diethyl ether
View Scheme
参考文献
CIBA
Patent: US2846382 , 1955 ;
反应条件
1: acetic acid / beim Erhitzen auf Siedetemperatur
2: lithium alanate; diethyl ether
3: ethanol
View Scheme
参考文献
CIBA
Patent: US2846382 , 1955 ;
反应条件
1: Ac2O / Heating
2: 79 percent / formamide / 0.05 h / microwave irradiation
3: 92 percent / dimethylformamide / 0.07 h / microwave irradiation
View Scheme
参考文献
Kacprzak, Karol
Synthetic Communications, 2003 , vol. 33, # 9 p. 1499 - 1507
反应条件
benzene
unter Entfernen des entstehenden Wassers;
参考文献
Teterin; Sonis
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 658,660
Chem. Zentralbl., 1936 , vol. 107, # II p. 2347
反应条件
sodium hydroxide; zinc in water
T=70 - 80°C; Dehalogenation; 6 h;
参考文献
Lee, Ho H.; Denny, William A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2755 - 2758
参考文献
Orndorff; Kennedy
Journal of the American Chemical Society, 1916 , vol. 38, p. 2487
反应条件
1: durch Trocknen im Vakuum ueber Phosphorpentoxyd
2: fuming sulfuric acid / 145 - 150 °C
View Scheme
参考文献
Orndorff; Black
American Chemical Journal, 1909 , vol. 41, p. 360,366
参考文献
Delbridge
American Chemical Journal, 1909 , vol. 41, p. 400,402, 406, 408, 409, 416
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Claus; Spruck
Chemische Berichte, 1882 , vol. 15, p. 1402
Full Text Show Details
Graebe
Justus Liebigs Annalen der Chemie, 1887 , vol. 238, p. 326,327
Chemische Berichte, 1883 , vol. 16, p. 861
