3,4,5,6-四氯-1,2-苯二甲酸半水合物合成路线 （共 50 条）
反应条件
1: Ac2O / Heating 2: 79 percent / formamide / 0.05 h / microwave irradiation View Scheme
参考文献
Kacprzak, Karol
Synthetic Communications, 2003 , vol. 33, # 9 p. 1499 - 1507
反应条件
1.1: Zn; NaOH / H2O / 6 h / 70 - 80 °C 2.1: Zn; NaOH / H2O / 5 h / 95 - 100 °C 3.1: toluene / Heating 4.1: KF; NaF / 130 - 270 °C / 20 Torr 4.2: NaCl; AlCl3 / 4 h / Heating View Scheme
参考文献
Lee, Ho H.; Denny, William A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2755 - 2758
反应条件
1.1: Zn; NaOH / H2O / 6 h / 70 - 80 °C 2.1: Zn; NaOH / H2O / 5 h / 95 - 100 °C 3.1: toluene / Heating 4.1: KF; NaF / 130 - 270 °C / 20 Torr 4.2: NaCl; AlCl3 / 4 h / Heating 4.3: pyridine / 58 h / 20 °C 5.1: 3-phenyl-2-(phenylsulfonyl)oxaziridine / CH2Cl2; methanol / 1 h / 0 °C View Scheme
参考文献
Lee, Ho H.; Denny, William A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 19 p. 2755 - 2758
反应条件
phosphorus; hydrogen iodide T=230°C; im geschlossenen Rohr;
参考文献
Graebe
Justus Liebigs Annalen der Chemie, 1887 , vol. 238, p. 326,327
Chemische Berichte, 1883 , vol. 16, p. 861
反应条件
T=230°C; im geschlossenen Rohr;
参考文献
Graebe
Justus Liebigs Annalen der Chemie, 1887 , vol. 238, p. 326,327
Chemische Berichte, 1883 , vol. 16, p. 861
参考文献
Graebe
Justus Liebigs Annalen der Chemie, 1905 , vol. 340, p. 247
反应条件
benzene
unter Entfernen des entstehenden Wassers;
参考文献
Teterin; Sonis
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 658,660
Chem. Zentralbl., 1936 , vol. 107, # II p. 2347
反应条件
1,2,3,4-tetrahydro-naphthalene
参考文献
Hodgson; Crook
Journal of the Chemical Society, 1936 , p. 1844,1846
反应条件
ethanol; hydrazine hydrate
T=140 - 150°C; mit l Mol Hydrazin-hydrat;
参考文献
Drew; Pearman
Journal of the Chemical Society, 1937 , p. 26,31
反应条件
1: acetic acid / beim Erhitzen auf Siedetemperatur
2: lithium alanate; diethyl ether
3: formamide
View Scheme
参考文献
Rosen et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 3167,3171
