1,1,3,3-四甲基脲合成路线 （共 85 条）
参考文献
Franchimont
Recueil des Travaux Chimiques des Pays-Bas, 1884 , vol. 3, p. 224
反应条件
(s-BuO)3Al in hexane; benzene byproducts: (C2H5)3GeGe(C2H5)3; to a degassed soln. of (s-BuO)3Al in hexane a soln. of Et3GeLi in benzene was added, pptn., addn. of (CH3)2NCON(CH3)2, mixt. shaken, hydrolysation after 15 min (react. also possible without alkoxide); product ratio detd. by GLC anal.;
参考文献
Seleznev, A. V.; Bravo-Zhivotovskii, D. A.; Vakul'skaya, T. I.; Voronkov, M. G.
Polyhedron, 1990 , vol. 9, p. 227 - 232
反应条件
sodium hydroxide in water T=25°C; hydrolytic decomposition; Rate constant;
参考文献
Kankaanperae, Alpo; Scharlin, Pirketta; Kuusisto, Ilona; Kallio, Riitta; Bernoulli, Emma
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 2 p. 169 - 174
反应条件
P=0.008 - 0.8 Torr; radio-frequency discharge; Yield given. Yields of byproduct given;
参考文献
Yajima, Tatsuhiko; Tsuchiya, Atsuhiko; Tezuka, Meguru
Tetrahedron Letters, 1987 , vol. 28, # 36 p. 4177 - 4178
反应条件
1: oxalyl chloride 2: KBF4,KCl View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 15 p. 1927 - 1930
反应条件
in monofluoro-trichloromethane T=-196.1°C; Irradiation;
参考文献
Symons, Martyn C. R.
Journal of the Chemical Society, Chemical Communications, 1986 , # 1 p. 11 - 12
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US4477389 A1, 1984 ;
反应条件
P=0.008 - 0.8 Torr; radio-frequency discharge; Yield given. Yields of byproduct given;
参考文献
Yajima, Tatsuhiko; Tsuchiya, Atsuhiko; Tezuka, Meguru
Tetrahedron Letters, 1987 , vol. 28, # 36 p. 4177 - 4178
反应条件
in benzene
T=140°C; 14 h; Product distribution;
参考文献
Bruni, Paolo; Conti, Carla; Tosi, Giorgio
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1311 - 1316
反应条件
T=195°C; Behandeln des Reaktionsprodukts mit LiAlH4 in Aether;
参考文献
Shaw
Journal of the American Chemical Society, 1955 , vol. 77, p. 4319,4320
Journal of the American Chemical Society, 1956 , vol. 78, p. 6419
