2-萘-1-基丙-2-醇合成路线 （共 29 条）
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in o-xylene 6 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 22 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
sodium tetrahydroborate; trifluoroacetic acid in tetrahydrofuran T=25°C; 1 h;
参考文献
Nutaitis, Charles F.; Bernardo, Joseph E.
Synthetic Communications, 1990 , vol. 20, # 4 p. 487 - 493
参考文献
Cook
Journal of the Chemical Society, 1932 , p. 456,470
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 4 h; Heating;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
反应条件
1: acetic acid anhydride 2: sulfur / 300 °C 3: KOH; CaO / 400 - 450 °C View Scheme
参考文献
Bergmann; Weizmann
Journal of Organic Chemistry, 1946 , vol. 11, p. 592,596
反应条件
1: ethylmagnesium bromide; methyllithium in tetrahydrofuran; diethyl ether
T=-78°C; 1 h;
2: methyl 1-naphthyl ketone in tetrahydrofuran; diethyl ether
T=-78°C; 5 h;
参考文献
Hatano, Manabu; Matsumura, Tokihiko; Ishihara, Kazuaki
Organic Letters, 2005 , vol. 7, # 4 p. 573 - 576
反应条件
in diethyl ether; toluene
T=0°C; 24 h; Inert atmosphere;
参考文献
Zhang, Jian; Yang, Nianfa; Yang, Liwen
Molecules, 2012 , vol. 17, # 6 p. 6415 - 6423
反应条件
1: 70 percent / perbenzoic acid / CHCl3 / 10 °C
2: LiAlH4
View Scheme
参考文献
Suprun
Advanced Synthesis and Catalysis, 1997 , vol. 339, # 7 p. 664 - 668
反应条件
in diethyl ether
2 h; Ambient temperature;
参考文献
Matsumoto; Takeda; Iwata; Sakamoto; Ishida
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 6 p. 1191 - 1197
