(S)-2-氨基-2-乙基己酸合成路线 （共 7 条）
反应条件
1: H2SO4 / Heating 2: 31 percent / porcine liver esterase / aq. phosphate buffer / 7.5 h / 30 °C / pH 8.0 View Scheme
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
反应条件
sulfuric acid Esterification; Heating;
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
反应条件
1: H2SO4 / Heating 2: porcine liver esterase / aq. phosphate buffer / 7.5 h / 30 °C / pH 8.0 View Scheme
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
反应条件
1: H2SO4 / Heating 2: 31 percent / porcine liver esterase / aq. phosphate buffer / 7.5 h / 30 °C / pH 8.0 3: NaOH / H2O / 21 h / 20 - 50 °C View Scheme
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
反应条件
hydrogenchloride
T=80°C; Hydrolysis; 24 h;
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
反应条件
1: NH4Cl / H2O; ethanol / 48 h / 55 - 60 °C
2: conc. HCl / 24 h / 80 °C
View Scheme
参考文献
Imawaka, Naoto; Tanaka, Masakazu; Suemune, Hiroshi
Helvetica Chimica Acta, 2000 , vol. 83, # 10 p. 2823 - 2835
参考文献
Abshire,C.J.; Planet,G.
Journal of Medicinal Chemistry, 1972 , vol. 15, p. 226 - 229
