N-甲基-3,4-二甲氧基苄胺合成路线 （共 9 条）
反应条件
1: in methanol T=20°C; 0.25 h; Inert atmosphere; 2: With sodium tetrahydroborate in methanol T=20°C; 1 h; Inert atmosphere;
参考文献
Castaing, Matthias; Wason, Sacha L.; Estepa, Beatriz; Hooper, Joel F.; Willis, Michael C.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 50 p. 13280 - 13283
Angew. Chem., 2013 , vol. 125, # 50 p. 13522 - 13525,4
反应条件
methylamine; palladium monocarbide in ethanol; water; toluene
反应条件
sodium tetrahydroborate in methanol T=0 - 20°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 16, # 5 p. 2499 - 2512
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Journal of Medicinal and Pharmaceutical Chemistry, , vol. 2, p. 617 - 631
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 9, p. 932
反应条件
titanium(IV) isopropylate; sodium tetrahydroborate; triethylamine 1.) EtOH, 25 deg C, 9 h, 2.) EtOH, 25 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 16 p. 2527 - 2531
参考文献
Journal of the American Chemical Society, , vol. 68, p. 201
反应条件
hydrogen bromide T=105°C; 5 h;
参考文献
Dalence-Guzman, Maria F.; Berglund, Magnus; Skogvall, Staffan; Sterner, Olov
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2499 - 2512
反应条件
1: H2O2; Na2WO4 / methanol / 1 h / 20 °C 2: hydroxylamine hydrochloride / methanol; diethyl ether / 4 h / 20 °C View Scheme
参考文献
Coskun, Necdet; Parlar, Aydin
Synthetic Communications, 2005 , vol. 35, # 18 p. 2445 - 2451
