Murray, Samuel M.; O'Brien, Richard A.; Mattson, Kaila M.; Ceccarelli, Christopher; Sykora, Richard E.; West, Kevin N.; Davis Jr., James H.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 15 p. 2755 - 2758
N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydride
1.) room temperature, THF 2.) room temperature for 16 h then 40 deg C for 2 h; Yield given. Multistep reaction;
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Thompson; Kraus
Journal of the American Chemical Society, 1947 , vol. 69, p. 1017
1: sodium; benzene / anschliessend Erhitzen ohne Loesungsmittel auf 150grad
2: nickel catalysts / 200 - 250 °C / 102971 - 117681 Torr / Hydrogenation
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参考文献
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Chem.Abstr., 1945 , p. 693
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