2,5-二甲基-1,5-己二烯合成路线 (共 92 条)
反应条件
magnesium 1) ether, 0 deg C --> rt, 30 h, rt, 2 h; 2) ether, THF, reflux, overnight; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 63, # 22 p. 7945 - 7952
参考文献
Tetrahedron Letters, , vol. 43, # 38 p. 6763 - 6766
反应条件
diethyl ether; magnesium
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 45, p. 947
Chem. Zentralbl., , vol. 84, # II p. 2104
反应条件
pyridine Destillation des durch Wasser gefaellten und mit Aether aufgenommenen Oeles unter vermindertem Druck;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 343, p. 366
反应条件
T=272°C; other temperature, heat of decomposition; thermolysis of 2,3-diazabicyclo<2.2.2>oct-2-ene derivatives; Rate constantThermodynamic data;
参考文献
Journal of the American Chemical Society, , vol. 105, # 24 p. 7102 - 7107
反应条件
tetrahydrofuran; sodium
参考文献
Chemische Berichte, , vol. 90, p. 543,549
反应条件
(i) nBuLi, THF, (ii) /BRN= 506525/, (iii) Ph3P; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 41, p. 1735 - 1742
Tetrahedron Letters, , p. 2861 - 2864
反应条件
in o-di-fluorobenzene Irradiationdirect and sensitized irradiation; photholysis of 2,3-diazobicyclo<2.2.2>oct-2-ene derivatives; fluorescence quantum yields and lifetimes, effect of temperature, rate constant for fluorescence; Product distributionThermodynamic dataQuantum yield;
参考文献
Journal of the American Chemical Society, , vol. 105, # 24 p. 7108 - 7114
参考文献
Journal of the American Chemical Society, , vol. 79, p. 3997,3999
反应条件
in diethyl ether 2.1 h in an argon atmosphere; gas-liquid chromy.;
参考文献
Theoretical and Experimental Chemistry, , vol. 26, p. 348 - 352
Teoreticheskaya i Eksperimental'naya Khimiya, , vol. 26, p. 371 - 375