4-(1,3-苯并噻唑-2-基)苯酚合成路线 （共 14 条）
反应条件
[C5mim](+)*Br(-) 0.0583333 h; microwave irradiation;
参考文献
Bandyopadhyay, Prabal; Sathe, Manisha; Prasad; Sharma, Pratibha; Kaushik
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 341, # 1-2 p. 77 - 82
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide T=80°C; 12 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C;
参考文献
Ma, Dawei; Xue, Peng; Jiang, Yongwen; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua
Angewandte Chemie, International Edition, 2009 , vol. 48, # 23 p. 4222 - 4225
反应条件
methanesulfonic acid; silica gel T=140°C; 3 h;
参考文献
Sharghi, Hashem; Asemani, Omid
Synthetic Communications, 2009 , vol. 39, # 5 p. 860 - 867
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide; toluene 2 h; Reflux;
参考文献
Weekes, Ashley A.; Frydrych, Jan; Westwell, Andrew D.
Synthetic Communications, 2013 , vol. 43, # 19 p. 2656 - 2662
反应条件
1-methyl-pyrrolidin-2-one; potassium carbonate; 2-amino-benzenethiol 0.25 h; Heating;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Nayak, Mrinal K.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6406 - 6414
反应条件
pyridine in ethanol; water; hydrogen bromide; acetic acid; benzene
反应条件
sulfur T=275°C; 0.5 h; Inert atmosphereAutoclave;
参考文献
Zhang, Li Fang; Ni, Zhong Hai; Li, Dong Ying; Qin, Zhi Hong; Wei, Xian Yong
Chinese Chemical Letters, 2012 , vol. 23, # 3 p. 281 - 284
反应条件
p-benozquinone in ethanol T=20°C; 1 h; Inert atmosphere;
参考文献
Monatshefte fur Chemie, , vol. 141, # 1 p. 45 - 48
反应条件
1: 90 percent / pyridine / 0.5 h / 25 °C 2: 56 percent / BBr3 / CH2Cl2 / 1.) -70 deg C, 1 h, 2.) from -70 deg C to 20 deg C, overnight View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 11 p. 1689 - 1695
反应条件
1: 90 percent / pyridine / 0.5 h / 25 °C 2: 56 percent / BBr3 / CH2Cl2 / 1.) -70 deg C, 1 h, 2.) from -70 deg C to 20 deg C, overnight View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 37, # 11 p. 1689 - 1695
