1,5-二苯基-1,5-戊二酮合成路线 （共 96 条）
反应条件
1: Me3SiNHSiMe3 / tetrahydrofuran 2: 2.) Bu4NF / 1.) THF, 2.) THF, H2O 3: 84 percent / CeCl3 / tetrahydrofuran / 12 h / 0 - 20 °C 4: 82 percent / t-BuOH, BuLi, CuBr2 / tetrahydrofuran; hexane / 1 h / Ambient temperature View Scheme
参考文献
Synlett, , vol. 1997, # 8 p. 962 - 964
反应条件
1: 84 percent / CeCl3 / tetrahydrofuran / 12 h / 0 - 20 °C 2: 82 percent / t-BuOH, BuLi, CuBr2 / tetrahydrofuran; hexane / 1 h / Ambient temperature View Scheme
参考文献
Synlett, , vol. 1997, # 8 p. 962 - 964
反应条件
1: 2.) Bu4NF / 1.) THF, 2.) THF, H2O 2: 84 percent / CeCl3 / tetrahydrofuran / 12 h / 0 - 20 °C 3: 82 percent / t-BuOH, BuLi, CuBr2 / tetrahydrofuran; hexane / 1 h / Ambient temperature View Scheme
参考文献
Synlett, , vol. 1997, # 8 p. 962 - 964
反应条件
1: 84 percent / CeCl3 / tetrahydrofuran / 12 h / 0 - 20 °C 2: 82 percent / t-BuOH, BuLi, CuBr2 / tetrahydrofuran; hexane / 1 h / Ambient temperature View Scheme
参考文献
Synlett, , vol. 1997, # 8 p. 962 - 964
反应条件
1: K2CO3 / methanol 2: 72 percent / manganese(III) 2-pyridinecarboxylate / dimethylformamide / 0 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 3 p. 819 - 827
反应条件
1: 91 percent / silica gel, H2O / CHCl3 / 3 h / Ambient temperature 2: 78 percent / K2CO3 / methanol / 8 h / Heating View Scheme
参考文献
Heterocycles, , vol. 31, # 9 p. 1699 - 1704
反应条件
anhydrous magnesium perchlorate; oxygen in acetonitrile 0.5 h; Irradiationsensitizer: DCA;
参考文献
Tetrahedron Letters, , vol. 35, # 23 p. 3953 - 3956
反应条件
aluminium trichloride T=0 - 20°C; Friedel-Crafts reaction; 12.5 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 71, # 9 p. 2181 - 2185
反应条件
1: Mg / diethyl ether / 4 h / Heating 2: SiO2/H2O View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 131, # 3 p. 247 - 252
反应条件
1: Mg / diethyl ether / 4 h / Heating 2: SiO2/H2O View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 131, # 3 p. 247 - 252
