lithium aluminium tetrahydride; aluminium trichloride in diethyl ether T=35°C; 0.25 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: With diMe-Imd-BH3; bis-(trifluoromethylsulphonyl)amine in dichloromethane T=20°C; 0.333333 h; Inert atmosphere; 2: With dihydrogen peroxide; sodium hydroxide in methanol; dichloromethane; water T=20°C; 16 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 29 p. 12281 - 12288
oxygen; [nBu4N][AuCl4] in dichloromethane T=15°C; 6 h; Irradiation;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 38, # 10 p. 2205
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2393
air; trans-lt;OsO2(CN)2(4,7-diphenyl-1,10-phenanthroline)gt; in dichloromethane; acetonitrile 12 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;