1: T=140°C;
2: With nickel; hydrazine hydrate in methanol
T=20°C; Leimgruber-Batcho reaction;
参考文献
Bentley, Jon M.; Davidson, James E.; Duncton, Matthew A. J.; Giles, Paul R.; Pratt, Robert M.
Synthetic Communications, 2004 , vol. 34, # 12 p. 2295 - 2300
1.1: HNO3; H2SO4 / -10 °C
2.1: NaNO2; aq. HCl / 0.33 h / 0 °C
2.2: 75 percent / aq. HCl; CuCl / 16 h / 0 - 20 °C
3.1: 140 °C
3.2: hydrazine hydrate; Raney nickel / methanol / 20 °C
View Scheme
参考文献
Bentley, Jon M.; Davidson, James E.; Duncton, Matthew A. J.; Giles, Paul R.; Pratt, Robert M.
Synthetic Communications, 2004 , vol. 34, # 12 p. 2295 - 2300
1.1: NaNO2; aq. HCl / 0.33 h / 0 °C
1.2: 75 percent / aq. HCl; CuCl / 16 h / 0 - 20 °C
2.1: 140 °C
2.2: hydrazine hydrate; Raney nickel / methanol / 20 °C
View Scheme
参考文献
Bentley, Jon M.; Davidson, James E.; Duncton, Matthew A. J.; Giles, Paul R.; Pratt, Robert M.
Synthetic Communications, 2004 , vol. 34, # 12 p. 2295 - 2300
