1,3-环氧-3-甲基丁烷合成路线 (共 11 条)
反应条件
1: 54 percent / conc. H2SO4 / dibutyl ether / 17 h / Ambient temperature 2: 50percent aq. KOH / 24 h / Heating View Scheme
参考文献
Gassman, Paul G.; Haberman, Leonard M.
Tetrahedron Letters, 1985 , vol. 26, # 41 p. 4971 - 4974
反应条件
zinc(II) chloride in 1,2-dichloro-ethane T=90°C; 24 h;
参考文献
Firgo, Heinrich A.; Weber, William P.
Journal of Organometallic Chemistry, 1981 , vol. 222, # 2 p. 201 - 210
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 20 p. 5760 - 5761
参考文献
Searles et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 948,950
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) Me2O, THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mudryk, Boguslaw; Cohen, Theodore
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5760 - 5761
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mudryk, Boguslaw; Cohen, Theodore
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5760 - 5761
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) Me2O, THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mudryk, Boguslaw; Cohen, Theodore
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5760 - 5761
反应条件
4,4'-di-tert-butylbiphenylide; triethylaluminum 1) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mudryk, Boguslaw; Cohen, Theodore
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5760 - 5761
参考文献
Bennett; Philip
Journal of the Chemical Society, 1928 , p. 1938
反应条件
sulfuric acid in anhydrous butyl ether
17 h; Ambient temperature;
参考文献
Pavel', T. M.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 157 - 159
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 1 p. 178 - 181