4-(2-呋喃基)-3-丁烯-2-酮合成路线 (共 89 条)
反应条件
palladium/alumina; hydrogen in carbon dioxide T=80°C; 20 h; Supercritical conditions;
参考文献
Green Chemistry, , vol. 12, # 5 p. 779 - 782
反应条件
1: ; hydrogen / tetrahydrofuran / 130 °C / 7500.75 Torr / Autoclave 2: / tetrahydrofuran / 175 °C / 18751.9 Torr View Scheme
参考文献
Xu, Wenjie; Xia, Qineng; Zhang, Yu; Guo, Yong; Wang, Yanqin; Lu, Guanzhong
ChemSusChem, 2011 , vol. 4, # 12 p. 1758 - 1761
反应条件
1: acetic acid anhydride; nitric acid / -30 °C View Scheme
参考文献
Wenter et al.
Latvijas PSR Zinatnu Akademijas Vestis, 1959 , # 8 p. 99,100, 103
Chem.Abstr., 1960 , p. 17363
Full Text Show Details
Eaton Labor. Inc.
Patent: US2599509 , 1950 ;
反应条件
1: H2 / Cu-chromit / dioxane / 230 °C / 228000 Torr 2: CrO3 / acetic acid View Scheme
参考文献
Thewalt,K.; Rudolph,W.
Journal fuer Praktische Chemie (Leipzig), 1964 , vol. 26, p. 233 - 261
反应条件
potassium fluoride; PdCl(C3H5)(dppb) in N,N-dimethyl acetamide T=130°C; 17 h; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2749 - 2760
反应条件
PdCl(C3H5)(dppb); caesium acetate in N,N-dimethyl acetamide T=130°C; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2749 - 2760
反应条件
potassium acetate; palladium diacetate; 1,4-di(diphenylphosphino)-butane in N,N-dimethyl acetamide T=130°C; regioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 14-15 p. 2749 - 2760
反应条件
ethanol; hydrazine hydrate
参考文献
Grandberg,I.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 2920 - 2925,2896 - 2900
反应条件
1: 86 percent / zinc chloride, triethylamine / acetonitrile / 5 h / 50 °C 2: 48 percent / toluene / 3 h / Heating View Scheme
参考文献
Tolstikov, G. A.; Shul'ts, E.E.; Safarova, G.M.; Spirikhin, L.V.; Panasenko, A.A.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 6 p. 1110 - 1119
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 6 p. 1283 - 1296
反应条件
sodium ethanolate Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 49, # 4 p. 900 - 904