n-butyllithium in diethyl ether addn. of ferrocene to BuLi (in hexanes/Et2O), refluxing for 6 h, stirring for 12 h, drpowise addn. of benzylhydroxylamine at -22°C, warming to room temp. (for 45 min); fractional extn. into 0.1 M HCl at 0°C, addn. of 12 M NaOH to last two extracts (crystn.), filtration, drying (vac.); (1)H-NMR spectroscopy;
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Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.1.1, page 4 - 6
Knox, G. R.; Pauson, P. L.
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Gmelin Handbook: Fe: Org.Verb.A4, 5.1.4.1.1.1, page 4 - 6
